Model of Steam and Water Extraction of Essential Oil of Eucalyptus Citriodora Using a Complete 2n Factorial Plan

Thomas Silou, Equipe Pluridisciplinaire de Recherche en Alimentation et Nutrition (EPRAN)
Georges Mapola, Service National de Reboisement, Congo
Roger Armand Makany, Equipe Pluridisciplinaire de Recherche en Alimentation et Nutrition (EPRAN)
Aubin Nestor Loumouamou, Equipe Pluridisciplinaire de Recherche en Alimentation et Nutrition (EPRAN)
Marc Malanda, Equipe Pluridisciplinaire de Recherche en Alimentation et Nutrition (EPRAN)
Jean-Claude Chalchat, Laboratoire de Chimie des Hétérocycles, des Glucides et des Huiles Essentielles,

Abstract

The steam and water distillation of leaves of Eucalyptus citriodora was modeled using a complete 2n factorial plan. Eight experiments were carried out, with three easily interpretable variables, for steam distillation and for a first degree polynomial model. The average essential oil yield was 2.3%. Positive effects decreased in the order: duration of the extraction, heating power and state of division of the plant. Interactions were negligible. Extraction conditions had no practical impact on citronellal content, which yielded an average content of 83.26% with a range of 80.2-85.4%. Weak negative effects were observed on duration of heating and state of division of plant material. Sixteen experiments were conducted on four variables for water distillation. The extracted essential oil yield was increased by 28%. Effects on citronellal content were the same as with steam extraction. Hence, water distillation is better suited for small-scale extraction given the simplicity of the equipment required and the significant gain in extraction yield.

Submitted: May 20, 2008 · Accepted: August 12, 2009 · Published: September 8, 2009

Recommended Citation

Silou, Thomas; Mapola, Georges; Makany, Roger Armand; Loumouamou, Aubin Nestor; Malanda, Marc; and Chalchat, Jean-Claude (2009) "Model of Steam and Water Extraction of Essential Oil of Eucalyptus Citriodora Using a Complete 2n Factorial Plan," International Journal of Food Engineering: Vol. 5 : Iss. 4, Article 9.
DOI: 10.2202/1556-3758.1442
Available at: http://www.bepress.com/ijfe/vol5/iss4/art9

 
 
 
 

ISSN: 1556-3758 ©1999-2009 The Berkeley Electronic Press™ All rights reserved.

To submit, subscribe, recommend this journal to your library, or sign up for email alerts, please visit: http://www.bepress.com/ijfe